The instrument used in the previous pages comprised the following components:
mini FloPro -1.5P
furnished with six position Valco valve and high flow rate Miligat pump,
configured to accommodate lab-on-valve module (A)
flow cell heater with electronic controller (B)
FloZF software, data acquisition and device control
Lab-on- valve
module with integrated flow cell and 600 micron quartz optical fibers encased
in 1.6mm O.D. PEEK sleeve.(C)
Holding coil heater
with electronic controller. The heater is furnished with 2 m long 0.8mm I.D. PEEK
tubing. The connecting tubing between heater and central port of LOV is only
5 cm long (volume 5 microliters). (D)
Tungsten light source, USB 4000 Spectrophotometer
Garth type flow cells ( 6cm (E) and 12cm (F) light path) were home made mainly
from Upchurch tubing and fittings.